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個(gè)人中心收藏查看我的收藏0有用+10消旋山莨菪堿播報(bào)討論上傳視頻藥品同義詞6542（6542）一般指消旋山莨菪堿消旋山莨菪堿，是一種有機(jī)化合物，化學(xué)式為C17H23NO4，主要用作抗膽堿藥。中文名消旋山莨菪堿 [3]
外文名Anisodamine
化學(xué)式C17H23NO4
分子量305.369
CAS登錄號(hào)17659-49-3
沸    點(diǎn)474.6 ℃
密    度1.3 g/cm3
閃    點(diǎn)240.8 ℃
是否納入醫(yī)保是
劑    型 口服常釋劑型； 注射劑 [3-4]
藥品類型 單方顛茄及其衍生物 [3-4]

目錄
1化合物簡(jiǎn)介?基本信息?理化性質(zhì)?分子結(jié)構(gòu)數(shù)據(jù)?計(jì)算化學(xué)數(shù)據(jù)2藥典信息?來(lái)源?性狀?鑒別?檢查?含量測(cè)定?類別?貯藏?制劑
化合物簡(jiǎn)介
播報(bào)編輯基本信息化學(xué)式：C17H23NO4分子量：305.369CAS號(hào)：17659-49-3理化性質(zhì)密度：1.3g/cm3沸點(diǎn)：474.6℃閃點(diǎn)：240.8℃折射率：1.600 [1]分子結(jié)構(gòu)數(shù)據(jù)摩爾折射率：82.30摩爾體積（cm3/mol）：240.4等張比容（90.2K）：661.0表面張力（dyne/cm）：57.1極化率（10-24cm3）：32.62 [1]計(jì)算化學(xué)數(shù)據(jù)疏水參數(shù)計(jì)算參考值（XlogP）：無(wú)氫鍵供體數(shù)量：2氫鍵受體數(shù)量：5可旋轉(zhuǎn)化學(xué)鍵數(shù)量：5互變異構(gòu)體數(shù)量：0拓?fù)浞肿訕O性表面積：70重原子數(shù)量：22表面電荷：0復(fù)雜度：396同位素原子數(shù)量：0確定原子立構(gòu)中心數(shù)量：4不確定原子立構(gòu)中心數(shù)量：1確定化學(xué)鍵立構(gòu)中心數(shù)量：0不確定化學(xué)鍵立構(gòu)中心數(shù)量：0共價(jià)鍵單元數(shù)量：1 [1]
藥典信息
播報(bào)編輯來(lái)源本品為(±)-6β-羥基-1αH,5αH-托烷-3α-醇托品酸酯，按干燥品計(jì)算，含C17H23NO4不得少于99.0%。性狀本品為白色結(jié)晶或結(jié)晶性粉末，無(wú)臭。本品在乙醇中易溶，在水中溶解，在0.01mol/L鹽酸溶液中溶解。熔點(diǎn)本品的熔點(diǎn)（通則0612）為103-113℃，熔距應(yīng)在6°C以內(nèi)。鑒別1、照薄層色譜法（通則0502）試驗(yàn)。供試品溶液：取本品，加甲醇制成每1mL中含3mg的溶液。對(duì)照品溶液：取消旋山茛若堿對(duì)照品，加甲醇制成每1mL中含3mg的溶液。色譜條件：采用硅膠GF254薄層板，以甲苯-丙酮-乙醇-濃氨溶液（4:5:0.6:0.4）為展開(kāi)劑。測(cè)定法：吸取上述兩種溶液各10μL，分別點(diǎn)于同一薄層板上，展開(kāi)，晾干，置紫外光燈（254nm）下檢視。結(jié)果判定：供試品溶液所顯主斑點(diǎn)的位置與顏色應(yīng)與對(duì)照品溶液的主斑點(diǎn)一致。2、本品的紅外光吸收?qǐng)D譜應(yīng)與對(duì)照的圖譜（光譜集811圖）一致。3、本品顯托烷生物堿類的鑒別反應(yīng)（通則0301）。檢查溶液的澄清度與顏色取本品0.50g，加水15mL溶解后，溶液應(yīng)澄清無(wú)色。有關(guān)物質(zhì)照高效液相色譜法（通則0512）測(cè)定。 供試品溶液：取本品，加0.01mol/L鹽酸溶液溶解并稀釋制成每1mL中約含1.5mg的溶液。對(duì)照品溶液：取雜質(zhì)Ⅰ對(duì)照品適量，加0.01mol/L鹽酸溶液溶解并稀釋制成每1mL中約含0.5mg的溶液。對(duì)照溶液：精密量取供試品溶液與對(duì)照品溶液各1mL，置100mL量瓶中，用0.01mol/L鹽酸溶液稀釋至刻度，搖勻。 色譜條件：用十八烷基硅烷鍵合硅膠為填充劑，以0.01mol/L磷酸二氫鉀溶液（含0.15%三乙胺，用磷酸調(diào)節(jié)pH值至6.5）-甲醇（70:30）為流動(dòng)相，檢測(cè)波長(zhǎng)為220nm，進(jìn)樣體積20μL。系統(tǒng)適用性要求：理論板數(shù)按消旋山茛若堿峰計(jì)算不低于2000，出峰順序依次為消旋山茛若堿順、反式異構(gòu)體與雜質(zhì)Ⅰ，消旋山茛若堿順、反式異構(gòu)體兩色譜峰之間的分離度應(yīng)符合要求。測(cè)定法：精密量取供試品溶液與對(duì)照溶液，分別注入液相色譜儀，記錄色譜圖至主成分峰保留時(shí)間的5倍。限度：供試品溶液色譜圖中如有雜質(zhì)峰，各雜質(zhì)峰面積的和（雜質(zhì)Ⅰ峰面積乘以校正因子0.44計(jì)）不得大于對(duì)照溶液中的消旋山茛若堿順、反式異構(gòu)體兩峰面積之和的1.5倍（1.5%）。干燥失重取本品，在60℃減壓干燥至恒重，減失重量不得過(guò)1.0%（通則0831）。含量測(cè)定取本品0.25g，精密稱定，加乙醇（對(duì)甲基紅指示液呈中性）5mL使溶解，精密加鹽酸滴定液（0.1mol/L）20mL，加甲基紅指示液1滴，用氫氧化鈉滴定液（0.1mol/L）滴定，并將滴定的結(jié)果用空白試驗(yàn)校正。每1mL鹽酸滴定液（0.1mol/L）相當(dāng)于30.54mg的C17H23NO4。類別抗膽堿藥。貯藏密封保存。制劑1、消旋山茛菪堿片。2、鹽酸消旋山茛菪堿注射液。 [2]新手上路成長(zhǎng)任務(wù)編輯入門編輯規(guī)則本人編輯我有疑問(wèn)內(nèi)容質(zhì)疑在線客服官方貼吧意見(jiàn)反饋投訴建議舉報(bào)不良信息未通過(guò)詞條申訴投訴侵權(quán)信息封禁查詢與解封?2024?Baidu?使用百度前必讀?|?百科協(xié)議?|?隱私政策?|?百度百科合作平臺(tái)?|?京ICP證030173號(hào)?京公網(wǎng)安備11000002000001號(hào)window.PAGE_DATA= 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